Documenta Praehistorica XL (2013) A new look at old material: ceramic petrography and Neo/Eneolithic pottery traditions in the eastern Ljubljansko barje, Slovenia Andreja ?ibrat Gašpari; Department of Archaeology, Faculty of Arts, University of Ljubljana, SI andreja.zibrat.gasparic@gmail.com ABSTRACT - In this article, a new look at old material, pottery, is presented, as the technology and operational sequences ofpottery from the Neolithic and Eneolithic in Slovenia is mostly understudied. Here, thefocus is on 5th and 4th millennia BC artefacts from the eastern part ofLjubljansko barje and sites, such as Resnikov prekop, Maharski prekop and Breg near Škofljica. The pottery was studied with a hand lens and petrographically, using an optical polarising microscope. The results were then compared to analyses of locally gathered clays and sediments. Pottery traditions at Resnikov prekop and Breg were different from those at Maharski prekop, although the vessels from all three sites were produced locally and mostly made from local material, but with different recipes or fabrics. The selection of raw material, the shaping and decorating ofpots, theirfiring and use were probably more related to different traditions and individual choices of potters at these sites than to purely technological choices. IZVLEČEK - V članku predstavljam nov pogled na star material, lončenino, saj se tehnologiji in operacijskim sekvencam pri izdelavi lončenine iz obdobja neolitika in eneolitika v Sloveniji posveča le majhna pozornost. Pričujoča analiza je osredotočena na artefakte 5. in 4. tisočletja BC. Iz vzhodnega dela Ljubljanskega barja, ki so bili izkopani na najdiščih Resnikov prekop, Maharski prekop in Breg pri Škofljici. Lončenino smo preiskali na makroskopskem nivoju in s petrografsko metodo opazovanja pod optičnim polarizacijskim mikroskopom. Rezultate smo primerjali z analizami lokalnih glin in sedimentov. Lončarske tradicije se na najdiščih Resnikov prekop in Breg razlikujejo od tradicij na Maharskem prekopu po svojih lončarskih masah in receptih, kljub temu da so bile posode izdelane iz lokalnih materialov. Izbor naravnih materialov, oblikovanje in okraševanjeposod, žganje in uporaba so verjetno povezani z različnimi tradicijami in individualnimi odločitvami lončarjev na teh najdiščih in ne prestavljajo izključno le tehnološke rešitve. KEY WORDS - Ljubljansko barje; Neolithic/Eneolithic; pottery technology; petrography; chaine ope-ratoire Introduction The Ljubljansko barje is a very intriguing place. This floodplain located to the south of the Slovenian capital, Ljubljana, has been a focus for archaeologists for more than a hundred years. In the Neolithic and Eneolithic, many settlements were erected on the floodplain, mostly in the tradition of so-called pile-dwellings, and these sites were present in this area at least from the 6th millennium calBC to the Early Bronze Age. Besides this long occupational sequence and similar building techniques, considerable differences may be observed in the material culture, especially in the different pottery traditions (e.g., Bre-gant 1964; Korošec 1964; Korošec, Korošec 1969; Bregant 1974a; 1974b; 1975; Harej 1975; 1978; 1981-82; 1987; Velušček 2004; 2006; 2009 etc.). Ljubljansko barje is also a subject of continuous debate over the existence or non-existence of a Holo-cene lake and the interpretation of Neolithic-Eneoli- DOI> 10.4312\dp.40.12 147 thic pile-dwellings (e.g., Melik 1946; Velušček 2004; 2007; Verbič 2011 contra Budja 1995; Mlekuž et al. 2006; Budja, Mlekuž 2008; 2010). Despite all the controversy surrounding these finds, the area has always been part of extensive studies covering many fields of research since the first excavations; from palynology to dendrochronology, from archaeozo-ology to material culture studies (e.g., Sercelj 1966; 1974; 1975; Strmole 1974; Osterc 1975; Stritar 1975; Golyeva 2006; Turk 2006; 2009; Bernardini 2009 etc.). With the vast scope of research it is surprising that the most common artefacts at these sites, namely pottery, are the most understudied material in terms of technology. Besides basic descriptions of colour, inclusions and general appearance, typological studies have been prevalent, and only some samples from Maharski prekop and Resnikov prekop have been studied with petrography and X-ray diffraction (Osterc 1975). In this article, a new look into old material, ceramics, is presented. The observations and results are based on studies of pottery samples from three Neolithic/ Eneolithic sites in Ljubljansko barje: Resnikov prekop, Maharski prekop and Breg near Škofljica. The samples were studied by hand specimen analysis and grouped according to their sand-sized inclusions. Later samples for were chosen for petrographical analysis, prepared as thin sections. The pottery was then ordered into various fabrics that can also be interpreted as the recipes of potters at these sites. In the last stage, these results were compared to analyses of locally gathered clays and sediments. The ceramic vessels are presented as part of an operational sequence or chaine operatoire in pottery preparation in the Neolithic and Eneolithic period of the eastern Ljubljansko barje region, and their role in the complexity of people's lives is also investigated. Archaeological sites and samples Resnikov prekop Resnikov prekop is one of the oldest Neolithic sites in central Slovenia and was discovered during excavations for a new canal near Ig on the Ljubljansko barje in 1953 (Fig. 1). In 1957, Stasko Jesse excavated two trenches, one on each side of the canal; the results of his excavation were published later, in the 1970s (Harej 1975). The most extensive excavations were carried out in 1962 by Josip Korošec (Bregant 1964; Korošec 1964). A small number of vertical and horizontal wooden piles was discovered, as well as fragments of branches, stone slabs and plaster fragments. A great amount of pottery, 8 stone axes and some silex tools were also found (Korošec 1964.34). In 2002, the Institute of Archaeology in Ljubljana excavated trenches at Resnikov prekop, south of Ko-rosec's excavation area, where mostly pottery was found (Velušček 2006). The excavation confirmed the observations from the 1960s that the cultural layer at the site had been swept away and the finds represent artefacts from different periods mixed together (Budja 1994/1995.167; Velušček 2006.57). Only heavier artefacts, such as pottery, stones, larger bones and vertical piles probably remained in their original positions at the site. The piles, although only a few of them have been excavated, show rows that ran in a southwest-northeast direction typical of Ljubljansko barje. In comparison with other so-called pile-dwelling sites on the Ljubljansko barje, Resnikov prekop has fewer piles and the buildings were poorly maintained. This led to the conclusion that the site was occupied for only a short period, perhaps less than a decade (Velušček 2006.57). According to the radiocarbon dates of vertical piles, the existence and duration of the Resnikov prekop site was placed firmly in the 46th century calBC (Cufar, Korenčič 2006.124, Tab. 2). Nevertheless, new radiocarbon dates from charred organic residues on pottery show that the occupation at Resnikov prekop had a longer time span, lasting from around 5300 to 4400 calBC (see Mlekuž et al. 2013). Maharski prekop This site was also discovered in 1953, at a location Na Mahu near the Maharski prekop canal (Fig. 1). Systematic excavations began in 1970 by Tatjana Bregant and the Department of Archaeology at the University in Ljubljana and continued for several seasons until 1977 (Bregant 1974a; 1974b; 1975; with unpublished material from seasons 1976and 1977). The excavated area was more than 1100m2 and the finds were documented in 4 x 4m grid squares (Bregant 1975.9-10). The results of these excavations and recent geomorphological assessments using LiDAR show that Maharski prekop is located on a flood-plain with several paleochannels and an active river channel near the site (Mlekuž et al. 2006; Budja, Mlekuž 2008). The site had a distribution of more than 2400 wooden piles, clay floors and grindstones, which were interpreted as the remains of 9 houses, approx. 4 x 10m in size (Mlekuž et al. 2006). New radiocarbon dates show that the occupation at Maharski prekop had roughly two phases: one dated between 4400 and 4000 calBC and the other between 3800 and 3550 calBC (Mlekuž et al. 2012.Fig. 2). Breg near Škofljica This site was discovered during a topographic survey and is located on a small isolated hill called Breg near the small town of Škofljica in the south-eastern part of Ljubljansko barje (Fig. 1). In the years 1983 to 1984 two small trenches, 2 x 2m, were excavated by Franc Osole and his team; the oldest layers were dated to the castelnovien or younger Mesolithic period (Frelih 1986.3536). The excavations yielded more than 2500 different stone tools, such as scrapers, blades, burins, cores and other types of flake (Frelih 1986.27). These layers were also radiocarbon dated, but the published dates are confusing, since different dates are given for the same samples (see Budja 1993175). The second excavation was led by Mihael Budja in the 1990s, and again two small trenches, 2 x 2m, were excavated (trench II in1996 and trench I in 1997). Pottery fragments were excavated in the oldest layer, together with typical Mesolithic geometrical tools (Tomaž 1999.58-73; Budja, Mlekuž 2008). Analytical methods To identify the pottery technology and the operational sequence or chaine operatoire, the pots were first sampled according to their stratigraphic position, vessel type and ornamentation techniques at each site. The samples were then analysed using a hand lens and following descriptions of pottery published by Milena Horvat (1999). Such hand specimen analyses enabled the characterisations of broader technological traits for large pottery assemblages. The basic composition of the pots was described, i.e. their inclusions, the abundance and size of the particles and the presence of voids; the hardness, surface colour, firing atmosphere and surface treatment were also recorded. The samples were then grouped into different fabric types, which enabled us to select samples for petrographic analysis. The petrogra-phic description of pottery enhances the identification of different non-plastic inclusions and allows for direct comparisons with regional geology (Whit-bread 2001.451). Pottery samples for the petrographic analysis were prepared as standard thin sections of 30|m thickness (Reedy 2008.1-3). The samples were then ana- Fig. 1. Map of the eastern part of Ljubljansko barje showing the locations of sites mentioned in the text: 1 Resnikov prekop; 2 Maharski prekop; 3 Breg near Škofljica; 4 Gornje mostišče. lysed under a polarising light microscope, following the descriptions proposed by Ian Whitbread (1995. Appendix 3) and the volume estimates were made using tables published by Richard D. Terry and George V. Chillingar (1955). The samples were then sorted into fabric groups, based on the composition of their inclusions, the clay matrix and the voids under the microscope. On the basis of compositional, microstructural and textural criteria, the presence of specific techniques was detected, such as the intentional addition of temper, raw material processing, vessel-forming techniques, and the atmosphere and degree of firing (Reedy 2008.146-148, 173189; Rice 1987.409-411; Whitbread 1986; 1995. 393-394). In addition, we sampled clays near Resnikov prekop and Maharski prekop. The clay samples were analysed using an X-ray diffractometer in their natural state, and were additionally prepared as approx. 3 x 4cm plates and fired in a controlled oxidising atmosphere at 700°C. The fired clay samples were then analysed using the X-ray diffraction technique, made into thin sections and analysed using a polarising light microscope, following a criteria similar to that applied to the pottery samples (Whitbread 1995; Terry, Chillingar 1952). Pottery technology at Resnikov prekop The most common types of vessel found at Resnikov prekop are various pots, followed by dishes, pedestal dishes, bowls, cups, jugs, and ladles with cylindrical handles (see Mlekuž et al. 2013). Vessel surfaces were smoothed or burnished, but no surface polishing was detected. These pots were made with the coiling technique, the walls are very fine and less than 5mm thick. The vessels were fired in an incomplete oxidising atmosphere, and only rare pots were fired in an oxidising and reducing atmosphere. The dominant colours of the pottery assemblage are grey, dark brown and light red (Korošec 1964.29-30; Ha-rej 1975.147; Tomaž, Velušček 2005.88-90). The most striking feature is the fact that all the ornamentation appears only on the exterior of the upper part of the vessels. The ornaments were made with impressions, incisions or appliques, or a combination of the three techniques. Some vessels were decorated with a red and, rarely, black slip, that was applied, unlike other ornamentation techniques, to the entire vessel, on the interior and exterior surfaces (Korošec 1964.33; Harej 1975.149; Velušček 2006.5758; Tomaž, Velušček 2005). For the present study, 120 pottery samples from Resnikov prekop were analysed with a hand lens for the presence of different inclusions, their size and frequency, and the presence of voids. The samples were chosen according to the typology of the published material from the site (Korošec 1964; Harej 1975; Velušček 2006) and were in part used also in the biochemical lipid analysis (see Mlekuž et al. 2013). These vessels could be attributed to three technological groups: the first group of vessels, made from non-calcareous clay and only quartz inclusions (31/120); the second group with quartz and calcite/ limestone inclusions is the most common (59/120); the third comprised mostly calcite/limestone inclusions (30/120). The majority of vessels, i.e. 52.5%, has inclusions in the size range of medium sand (0.25 to 0.50mm) and a further 40.8% has inclusions in the range of very fine sand (less than 0.25mm). Vessels with coarser sand inclusions (0.50 to 2.00mm) are much less common (6.7%) and made mostly with quartz and calcite/limestone inclusions belonging to the second technological group. Various pots, different types of dishes and pedestal dishes from Resnikov prekop share many technological characteristics and are typically made with inclusions of quartz and calcite/limestone, which are in the medium sand fraction. Different types of bowl are similarly made, but nevertheless exhibit a stronger presence of vessels made only with quartz inclusions and much more fine-grained fabrics, with fine sand inclusions. Petrographic analysis of the Resnikov prekop pottery For the petrographic analysis of pottery from Resni-kov prekop, 25 samples were chosen and prepared as standard thin sections (Tab. 1). All samples were chosen according to the technological characteristics observed in the hand specimen description (see above) covering all the different technological groups. These samples can be attributed to eight different fabric groups according to the characteristics of clays and inclusions, as well as temper added by the potters at Resnikov prekop (Tab. 2, Fig. 2). Fabric RP-1 (Fig. 2.A) is a very fine-grained non-calcareous clay with frequent (40%) non-plastic inclusions, with a few sponge spicules present in the paste. The clay appears to be only cleaned of coarser inclusions and no temper was added. The inclusions are well sorted and mostly in the silt size fraction. The inclusions are frequent monocrystalline quartz, frequent muscovite and very rare biotite mica, a few sponge spicules, rare chert grains, common opaques or 'amorphous' concentration features (see Whitbread 1995.386) and very rare feldspars-plagioclase grains (Tab. 2). The fabric could be identified in three samples from the Jesse trench I excavated in 1957 (Harej 1975), but was not present in any of the other trenches. Fabric RP-2 (Fig. 2.B) is also a very fine-grained non-calcareous clay, with common (20%) non-plastic inclusions with frequent opaques. The clay was only cleaned of coarser inclusions, since no temper was added by the potters. The inclusions are mostly well sorted and have grains in the silt size fraction. The inclusions are frequent monocrystalline quartz, rare chert grains, common muscovite and a few biotite mica, with very rare sandstone grains and very rare argillaceous rock fragments (see Whitbread 1986) (Tab. 2). The fabric was identified in five samples from all excavated trenches and came from vessels such as pots, dishes and pedestal vessels (e.g., Korošec 1964.T. 10.7). Fabric RP-3 (Fig. 2.C) has a coarser texture and is a non-calcareous clay with common (20%) non-plastic inclusions and chert, probably added as temper. The chert grains are common (10%), semi-angular and medium sorted, mostly in the fine to medium sand fraction, and could have been added as temper by the potters. The other inclusions include frequent monocrystalline quartz, frequent muscovite and very rare biotite mica, a few opaques and very rare argillaceous rock fragments (Tab. 2). The fabric could be Sample Site Year of Grid Context Vessel type Fabric Citation No. excavation square group RP5 Resnikov prekop 1957 deep dish RP-5 Harej 1975.T. 2.10 RP15 Resnikov prekop 1957 pot RP-2 Harej 1975.T. 6.8 RP20 Resnikov prekop 1957 Trench 1 small pot RP-1 Not published RP21 Resnikov prekop 1957 Trench 1 small pot RP-1 Not published RP22 Resnikov prekop 1957 Trench 1 cup RP-1 Not published RP23 Resnikov prekop 1957 Trench 1 small pot RP-2 Not published RP24 Resnikov prekop 1957 Trench 1 pot RP-5 Not published RP30 Resnikov prekop 1962 pot RP-5 Korošec 1964.T. 18.1 RP34 Resnikov prekop 1962 bowl RP-8 Not published RP35 Resnikov prekop 1962 pedestal dish RP-3 Not published RP44 Resnikov prekop 1962 dish RP-2 Korošec 1964.T. 10.7 RP50 Resnikov prekop 1962 pedestal dish RP-6 Korošec 1964.T. 15.4 RP73 Resnikov prekop 1962 bowl? RP-8 Not published RP79 Resnikov prekop 2002 11 Trench 1/SU 005 pot RP-8 Not published RP84 Resnikov prekop 2002 9 Trench 1/SU 005 pot RP-5 Not published RP85 Resnikov prekop 2002 4 Trench 2/SU 005 pot RP-6 Velušček 2006.T. 13.3 RP89 Resnikov prekop 2002 11 Trench 1/SU 005 pedestal vessel RP-2 Not published RP91 Resnikov prekop 2002 11 Trench 1/SU 005 pot RP-7 Not published RP92 Resnikov prekop 2002 1 Trench 2/SU 005 pedestal vessel RP-5 Not published RP98 Resnikov prekop 2002 9 Trench 3/SU 005 pedestal dish RP-6 Velušček 2006.T. 19.4 RP100 Resnikov prekop 2002 9 Trench 3/SU 005 bowl RP-8 Velušček 2006.T. 19.1 RP107 Resnikov prekop 2002 8 Trench 3/SU 005 pot RP-6 Not published RP108 Resnikov prekop 2002 8 Trench 3/SU 005 pot RP-2 Not published RP110 Resnikov prekop 2002 7 Trench 2/SU 005 deep dish RP-7 Velušček 2006.T. 15.1 RP111 Resnikov prekop 2002 7 Trench 2/SU 005 dish RP-4 Velušček 2006.T. 14.18 MP22 Maharski prekop 1974 17 pot MP-1 Bregant 1975.T. 15.4 MP26 Maharski prekop 1973 18 pot MP-1 Bregant 1975.T. 16.1 MP47 Maharski prekop 1973 23 pot MP-1 Bregant 1975.T. 22.6 MP55 Maharski prekop 1973 24 pot MP-1 Bregant 1975.T. 23.9 MP79 Maharski prekop 1974 27 dish MP-1 Bregant 1975.T. 29.2 MP103 Maharski prekop 1974 37 pot MP-1 Bregant 1975.T. 35.10 MP104 Maharski prekop 1974 37 pot MP-1 Bregant 1975.T. 36.2 MP199 Maharski prekop 1977 71 bowl MP-1 Not published MP206 Maharski prekop 1970 1-8 bowl MP-1 Not published MP211 Maharski prekop 1970 1-8 pot MP-1 Not published MP13 Maharski prekop 1972 13 pot MP-2 Bregant 1974b.T6.17 MP133 Maharski prekop 1972 13 pot MP-2 Not published MP147 Maharski prekop 1976 44 pot MP-3 Not published MP148 Maharski prekop 1976 44 pot MP-3 Not published MP185 Maharski prekop 1977 68 pot MP-4 Not published BR1 Breg near Škofljica 1997 3 SU 06 pot B-1 Tomaž 1999.T. B1.9 BR5 Breg near Škofljica 1997 3 SU 07 pot B-3 Not published BR6 Breg near Škofljica 1997 4 SU 03/3 pot B-2 Not published BR7 Breg near Škofljica 1997 4 SU 07 pot B-1 Not published Tab. 1. List of pottery and clay samples presented in the article. identified in only one thin section from a deep dish, with an applique from Korosec's trench (unpublished, similar to Korošec 1964.T. 7.1). Fabric RP-4 (Fig. 2.D) has a fine texture and is a non-calcareous clay with a few (10%) non-plastic inclusions and chert, probably added as temper. The chert grains are common, semi-angular and medium sorted, mostly in the sand fraction up to 1.5 mm, and could have been added as temper by the potters. The other inclusions include frequent monocrystal-line quartz, very rare sandstone grains, a few muscovite and very few biotite mica, a few opaques and very few clay pellets (Tab. 2). The fabric could be identified in only one thin section from a bowl from trench 2, excavated in 2002 (Velušček 2006.T. 14. 18). Fabric RP-5 (Fig. 2.E) is a coarsegrained non-calcareous clay with frequent (30-40%) non-plastic inclusions. The inclusions are medium sorted, and especially quartz, sandstone and limestone grains are in the medium to coarse sand and even gravel fraction (more than 2mm). The inclusions include dominant mo-nocrystalline quartz, frequent muscovite and very few biotite mica, very few sandstone and calcareous sandstone, very rare limestone, very few chert, a few opaques and very rare plagioclase feldspars (Tab. 2). It is not clear if the coarse quartz, sandstone, calcareous sandstone and limestone grains were intentionally added to the clay as temper, since the overall fabric and opaques or 'amorphous' concentration features can also be quite coarse in these samples. The samples made with this fabric come mostly from pots, as well as from pedestal vessels and bowls with a red slip (e.g., Harej 1975.T. 2.10). Fabric RP-6 (Fig. 2.F) is a non-calcareous clay with a few (10%) non-plastic inclusions. The inclusions are predominantly monocrystalline quartz, common muscovite and very few biotite mica, very few limestone grains, rare sandstone and chert, common opaques and very rare pla-gioclase feldspars (Tab. 2). The quartz, sandstone and chert grains are well sorted and mostly in the silt to fine sand fraction, and limestone grains are medium to poorly sorted, in the medium to coarse sand fraction. Limestone could have been added as temper to the clay paste according to the size, shape and sorting of the grains. The fabric is present in dishes, pedestal dishes and pots (Korošec 1964.T. 15.4; Velušček 2006.T. 13.3, T. 19.4). Fabric RP-7 (Fig. 2.G) is a non-calcareous clay with common (20%) non-plastic inclusions The inclusions are well to medium sorted and mostly in the silt fra- Fig. 2. Photomicrographs of the petrographic fabric groups detected at Resnikov prekop: A - fabric group RP-1; B - fabric group RP-2; C - fabric group RP-3; D - fabric group RP-4; E - fabric group RP-5; F - fabric group RP-6; G - fabric group RP-7; H - fabric group RP-8. Images A-B taken in plane polarised light; image width is 1mm. Images C-H taken in crossedpolars; image width is 2mm (photo by the author). ction; the quartz and limestone grains can be up to coarse sand fraction. The inclusions are predominantly monocrystalline quartz, common limestone, few muscovite and rare biotite mica, rare sandstone, very rare chert, very rare plagioclase feldspars and a few opaque grains (Tab. 2). The limestone is sub-rounded, well sorted and mostly in silt-size fractions, meaning it is a natural inclusion in the clay paste. The fabric is typical of dishes and pots, and found only in vessels excavated in Velušček's trench (e.g., Velušček 2006.T. 15.1). Tab. 2. The basic mineralogical composition of the eight fabric groups typical of the Resnikov prekop pottery. Fabric Sample No. Calcite Limestone Sandstone Spicules Quartz Chert Muscovite Biotite Opaques groups (in %) (in %) (in %) (in %) (in %) (in %) (in %) (in %) (in %) Fabric RP- -1 RP20,RP21,RP22 0 0 0 5-15 30-35 0.5-2 35-4° <°.5 10-25 Fabric RP -2 RPi5,RP23,RP44, RP89,RPIO8 0 0