12 A. I. Aydeniz, A. Göksenli, G. Dil, F. Muhaffel, C. Calli, B. Yüksel, Electroless Ni-B-W Coatings for Improving Hardness, Wear And Corrosion Resistance, MTAEC9, 47 (2013) 6, 803–806 13 T. S. N. Sankara Narayanan, K. Krishnaveni, S. K. Seshadri, Elec- troless Ni–P/Ni–B Dublex Coatings: Preparation and Evaluation of Microhardness, Wear and Corrosion Resistance, Mater. Chem. Phys., 82 (2003), 771–779, doi:10.1016/S0254-0584(03)00390-0 14 W. X. Zhang, Z. H. Jiang, G. Y. Li, Q. Jiang, J. S. Lian, Electroless NiP/NiB Dublex Coatings For Improving The Hardness and The Corrosion Resistance of AZ91 D Magnesium Alloy, Appl. Surf. Sci., 254 (2008), 4949–4955, doi:10.1016/j.apsusc.2008.01.144 15 A. B. Drovosekov, M.V. Ivanov, V. M. Krutskikh, E. N. Lubnin, Y. M. Polukarov, Chemically Deposited Ni-W-B Coatings: Composi- tion, Structure and Properties, Prot. Met., 41(2005) 1, 55–62, doi:10.1007/s11124-005-0008-1 16 F. Z. Yang, Z. H. Ma, L. Huang, S. K. Xu, S. M. Zhou, Electro- deposition and Properties of an Amorphous Ni-W-B Alloy before and after Heat Treatment, Chin. J. Chem., 24 (2006), 114–118, doi:10.1002/cjoc.200690004 17 S. Ruan, C. A. Schu, Mesoscale Structure and Segregation in Electrodeposited Nanocrystalline Alloys, Scripta Mater., 59 (2008) 11, 1218–1221, doi:10.1016/j.scriptamat.2008.08.010 18 R. A.C. Santana, S. Prasad, A. R. N. Campos, F. O. Arau´ jo, G.P. Sýlva, P. Lima-Neto, Electrodeposition and Corrosion Behaviour of a Ni–W–B Amorphous Alloy, J. Appl. Electrochem., 36 (2006), 105–113, doi:10.1007/s10800-005-9046-2 19 R. A. Yildiz, A. Göksenli, B. Yüksel, F. Muhaffel, A. Aydeniz, Effect of Annealing Temperature on The Corrosion Resistance of Elec- troless Produced Ni-B-W Coatings, Adv Mat Res., 652 (2013), 263–268, doi:10.4028/www.scientific.net/AMR.651.263 20 Z. Z. Hamid, H. B. Hassan, A. M. Attyia, Influence of Deposition Temperature and Heat Treatment on The Performance of Electroless Ni–B Films, Surf. Coat. Technol., 205 (2010) 7, 2348–2354, doi:10.1016/j.surfcoat.2010.09.025 B. YÜKSEL et al.: CORROSION RESISTANCE OF AS-PLATED AND HEAT-TREATED ELECTROLESS ... 842 Materiali in tehnologije / Materials and technology 51 (2017) 5, 837–842 MATERIALI IN TEHNOLOGIJE/MATERIALS AND TECHNOLOGY (1967–2017) – 50 LET/50 YEARS J. ZHE et al.: SHORT-TERM CREEP OF P91 HEAT-RESISTANT STEELS AT LOW STRESSES ... 843–847 SHORT-TERM CREEP OF P91 HEAT-RESISTANT STEELS AT LOW STRESSES AND AN INSTANTANEOUS-STRESS-CHANGE TESTING KRATKOTRAJNO LEZENJE TOPLOTNO ODPORNEGA JEKLA P91 PRI NIZKIH NAPETOSTIH IN NENADNI MENJAVI NAPETOSTI OBREMENJEVANJA Jiang Zhe, Shen Junjie, Zhao Pengshuo Tianjin University of Technology, Tianjin Key Laboratory for Advanced Mechatronic System Design and Intelligent Control, National Demonstration Center for Experimental Mechanical and Electrical Engineering Education, 391 Binshui Road, Xiqing District, Tianjin, China sjj1982428@sina.com, j211209977@live.com Prejem rokopisa – received: 2016-1'-20; sprejem za objavo – accepted for publication: 2017-03-21 doi:10.17222/mit.2016.305 For the short-term creep behavior to be evaluated and the creep mechanism of P91 heat-resistant steels at low stresses and high temperatures to be clarified, stress-change testing was conducted with a “helicoidal-spring creep test” demonstrating a high strain resolution. The creep deformation consists of the primary creep stage, whereas no secondary creep stage was observed. Blackburn’s law was suggested to be the best choice for a short-term-creep-behavior description because it provides a good representation of an experimental creep curve. An anelastic backflow at a low stress was confirmed, following a high reduction in the stress. The absolute value of the instantaneous strain for a load increase was equal to the value for a load decrease and the creep of the P91 steels at low stresses might have been controlled by the viscous glide of dislocations. Keywords: P91 heat-resistant steel, creep, anelastic, stress change Da bi bilo mo~ oceniti kratkotrajno lezenje in njegov mehanizem toplotno obstojnega jekla P91 pri nizkih napetostih in visokih temperaturah, so bili izvedeni preizkusi spremembe napetosti z uporabo t.i. testa spiralne vzmeti, ki omogo~a veliko lo~ljivost deformacije. Deformacija lezenja sestoji iz primarne in sekundarne faze lezenja, vendar sekundarne faze niso analizirali oz. opazovali. Blackburnov zakon je najbolj uporaben zakon za opis obna{anja jekla med kratkotrajnim lezenjem, ker se z njim najbolj pribli`amo rezultatom, dobljenim z eksperimenti. Neelasti~ni povratni tok pri nizki napetosti je bil potrjen z ve~jim zmanj{anjem napetosti. Zaradi absolutne vrednosti trenutne deformacije za dano obremenitev je bil narastek deformacije enak zmanj{anju obremenitve, medtem ko je lezenje pri nizkih napetostih jekla P91 kontrolirano z viskoznim drsenjem dislokacij. Klju~ne besede: P91 jeklo za delo v vro~em, lezenje, neelasti~nost, sprememba napetosti 1 INTRODUCTION The P91 ferritic heat-resistant steel is utilized for the material production of thermal-power-plant components, which are exposed to elevated temperatures for extensive periods. This requires that the P91 structural materials resist creep deformation at both high temperatures and low stresses. The creep strength obtained with the extra- polation method based on the data of the creep deforma- tion at a high stress is higher than the true creep strength under these conditions (at low stresses).1,2 The creep- strength degradation is not only based on the microstruc- tural degradation3–6, but it is also related to the change in the creep mechanism.7–9 The creep-mechanism clarifica- tion has to depend on the instantaneous creep behavior because the long-term creep is associated with the micro- structural degradation. The stress-change test constitutes an effective method for a creep-deformation-mechanism clarification based on the instantaneous-strain and creep-rate-variation evaluation at the stress changes during the creep testing.10–12 At a high strain rate (a high stress) and a high tem- perature, a sudden-stress-change experiment has been widely utilized for pure metals and solution-strengthened alloys.10–12 In contrast, at a low strain rate 0, especially the ultra-low 0, lower than 10–10 s–1, it is usually impossi- ble for a conventional tension-creep technique to dist- inguish the instantaneous plastic strain from the total strain under a sudden stress change, due to the unsatis- factory strain resolution, existing between 10–6 and 10–5. As an additional creep technique, the helicoidal-spring creep test based on torsion deformation provides a significantly high strain resolution, even up to 10–9.13 Due to this high strain resolution, it is possible for very low instantaneous strains to be measured during a sudden stress change.14 In the present study, the instantaneous creep of the P91 ferritic heat-resistant steels was studied during sudden-stress-change experiments using the helicoidal- spring-specimen technique for the creep mechanism under both a low stress and a high temperature. Materiali in tehnologije / Materials and technology 51 (2017) 5, 843–847 843 MATERIALI IN TEHNOLOGIJE/MATERIALS AND TECHNOLOGY (1967–2017) – 50 LET/50 YEARS UDK 621.9.011:620.172.24:691.714 ISSN 1580-2949 Original scientific article/Izvirni znanstveni ~lanek MTAEC9, 51(5)843(2017) 2 EXPERIMENTAL PART 2.1 Materials The P91 heat-resistant steel was utilized in this expe- riment. The chemical components are presented in Table 1. 2.2 Specimen processing The steel was processed into helicoidal-spring speci- mens using the method of high-speed wire-electrode cutting machining; the outer and inner diameters of the specimens were 12 mm and 8 mm, respectively. The cross-section of the helicoidal-spring specimens was a rectangle. The side length of the rectangle was 2 mm, as presented in Figure 1. The helicoidal-spring specimens were annealed at 1313 K for 60 min and consequently tempered at 1033 K for 60 min. 2.3 Test methods Figure 2 presents the experimental apparatus, which includes an electric furnace with three adjacent heaters, a high-precision optical micrometer, a load, a weight and a system for receiving and processing information. By measuring the helicoidal-spring-specimen pitch change, the creep curves could be obtained. The test-apparatus details were previously reported.14 During the testing, the number of weights was in- creased or decreased for the instantaneous stress change to be observed. The weight was suspended under a load with a flammable thread. In order for a load to be increased, the load was hooked quickly. For a load to be decreased, the flammable thread was burned. The test was performed at a temperature of 923 K and a slight oscillation. The specimen was loaded sub- sequently for five days when the strain rate was down to 10–9–10–8 s–1. Also, the stress consequently increased or decreased at various applied levels and the instantaneous strain was measured. The following equations15,16 were utilized for calculating the mean surface shear stress, , and the surface shear strain, , with the assumption of the pure torsion of the helicoidal-spring specimen:  = PD a b2 2 (1)  = 2 2 a Dπ Δ (2) where P is the average load, D is the coil diameter (12 mm) and  is the displacement of the mean coil-pitch spacing. In this study, the torsion was the dominant component of deformation, because D was quite higher than d (D/d > 12)17 and the value of was between 2 mm and 4 mm.18 Since the stress and strain in the helicoidal spring had essentially shear components, the former could be transformed into the equivalent tensile quantities with the von Mises equations for the tensile stress  = 3 and the tensile strain  = / 3. 3 RESULTS AND DISCUSSION Figure 3 demonstrates the creep curves obtained at 923 K and at various stresses: (34.85, 27.75 and 19.35) MPa. J. ZHE et al.: SHORT-TERM CREEP OF P91 HEAT-RESISTANT STEELS AT LOW STRESSES ... 844 Materiali in tehnologije / Materials and technology 51 (2017) 5, 843–847 MATERIALI IN TEHNOLOGIJE/MATERIALS AND TECHNOLOGY (1967–2017) – 50 LET/50 YEARS Table 1: Chemical components of P91 Element Cr Mo Si V C Nb Cu N P Ni Ti Al S Content (%) 9.50 0.91 0.60 0.20 0.10 0.10 0.07 0.04 0.02 0.02 0.01 0.01 0.01 Figure 2: Experimental apparatus including electric furnace, high- precision optical micrometer, load, weight and information-receiving and processing systemFigure 1: Helicoidal-spring specimen for the stress-change testing The creep rate which corresponded to the slope of the curves decreased as the duration increased. Figure 4 presents the strain rate on a logarithmic plot versus the strain at 923 K and various stresses. The creep deformation of the P91 steels consisted of the primary creep stages where the creep rate decreased along with the strain and no apparent secondary (steady-state) creep stage was observed where the creep rate would not change along with the strain. The constitutive creep equations expressing the pri- mary stages should be utilized in the experimental creep-curve analysis. The following constitutive creep equations were utilized, being widely accepted as the basic creep equations.19,20 Power law:  = 0 + at b (3) Exponential law:  = 0 + a[1-exp(-bt)] (4) Logarithmic law:  = 0 + a ln(1+bt) (5) Blackburn’s law:  = 0 + ac[1 - exp(-bt)]+c[1 - exp(-dt)] (6) where  is the strain, 0 is the instantaneous strain on dead weight, t is the elapsed time and a, b, c and d are the parameters characterizing the primary creep region. The a, b, c and d values were called the "scaling fac- tors".21 Figure 5 presents representative results of a re- gression analysis, for the creep at 923 K and 27.75 MPa. The exponential-law and power-law equations did not reproduce the experimental data. Compared to the loga- rithmic-law equation, the Blackburn equation provided a better representation of the experimental creep curve. Therefore, the short-term creep for the P91 heat-resistant steels at low stresses could be described with the Blackburn equation. In order for the creep mechanism of the P91 steels at low stresses to be studied, the instantaneous creep behavior was investigated. The specimens were loaded for 4.3 × 105 s until the strain reached 6 × 10–3. In this case, the dislocations could be expected to move. The stress increased or decreased at various levels that were consequently applied and the instantaneous strain was measured. J. ZHE et al.: SHORT-TERM CREEP OF P91 HEAT-RESISTANT STEELS AT LOW STRESSES ... Materiali in tehnologije / Materials and technology 51 (2017) 5, 843–847 845 MATERIALI IN TEHNOLOGIJE/MATERIALS AND TECHNOLOGY (1967–2017) – 50 LET/50 YEARS Figure 3: Strain/time creep curves for P91 at 923 K and various stresses Figure 4: Strain rate/strain creep curves at 923 K and various stresses Figure 6: Example of instantaneous elongation and contraction upon low stress changes at a high temperature Figure 5: Comparison of experimental data and predicted curves of strain versus time at 923 K and 27.75 MPa 2 EXPERIMENTAL PART 2.1 Materials The P91 heat-resistant steel was utilized in this expe- riment. The chemical components are presented in Table 1. 2.2 Specimen processing The steel was processed into helicoidal-spring speci- mens using the method of high-speed wire-electrode cutting machining; the outer and inner diameters of the specimens were 12 mm and 8 mm, respectively. The cross-section of the helicoidal-spring specimens was a rectangle. The side length of the rectangle was 2 mm, as presented in Figure 1. The helicoidal-spring specimens were annealed at 1313 K for 60 min and consequently tempered at 1033 K for 60 min. 2.3 Test methods Figure 2 presents the experimental apparatus, which includes an electric furnace with three adjacent heaters, a high-precision optical micrometer, a load, a weight and a system for receiving and processing information. By measuring the helicoidal-spring-specimen pitch change, the creep curves could be obtained. The test-apparatus details were previously reported.14 During the testing, the number of weights was in- creased or decreased for the instantaneous stress change to be observed. The weight was suspended under a load with a flammable thread. In order for a load to be increased, the load was hooked quickly. For a load to be decreased, the flammable thread was burned. The test was performed at a temperature of 923 K and a slight oscillation. The specimen was loaded sub- sequently for five days when the strain rate was down to 10–9–10–8 s–1. Also, the stress consequently increased or decreased at various applied levels and the instantaneous strain was measured. The following equations15,16 were utilized for calculating the mean surface shear stress, , and the surface shear strain, , with the assumption of the pure torsion of the helicoidal-spring specimen:  = PD a b2 2 (1)  = 2 2 a Dπ Δ (2) where P is the average load, D is the coil diameter (12 mm) and  is the displacement of the mean coil-pitch spacing. In this study, the torsion was the dominant component of deformation, because D was quite higher than d (D/d > 12)17 and the value of was between 2 mm and 4 mm.18 Since the stress and strain in the helicoidal spring had essentially shear components, the former could be transformed into the equivalent tensile quantities with the von Mises equations for the tensile stress  = 3 and the tensile strain  = / 3. 3 RESULTS AND DISCUSSION Figure 3 demonstrates the creep curves obtained at 923 K and at various stresses: (34.85, 27.75 and 19.35) MPa. J. ZHE et al.: SHORT-TERM CREEP OF P91 HEAT-RESISTANT STEELS AT LOW STRESSES ... 844 Materiali in tehnologije / Materials and technology 51 (2017) 5, 843–847 MATERIALI IN TEHNOLOGIJE/MATERIALS AND TECHNOLOGY (1967–2017) – 50 LET/50 YEARS Table 1: Chemical components of P91 Element Cr Mo Si V C Nb Cu N P Ni Ti Al S Content (%) 9.50 0.91 0.60 0.20 0.10 0.10 0.07 0.04 0.02 0.02 0.01 0.01 0.01 Figure 2: Experimental apparatus including electric furnace, high- precision optical micrometer, load, weight and information-receiving and processing systemFigure 1: Helicoidal-spring specimen for the stress-change testing The creep rate which corresponded to the slope of the curves decreased as the duration increased. Figure 4 presents the strain rate on a logarithmic plot versus the strain at 923 K and various stresses. The creep deformation of the P91 steels consisted of the primary creep stages where the creep rate decreased along with the strain and no apparent secondary (steady-state) creep stage was observed where the creep rate would not change along with the strain. The constitutive creep equations expressing the pri- mary stages should be utilized in the experimental creep-curve analysis. The following constitutive creep equations were utilized, being widely accepted as the basic creep equations.19,20 Power law:  = 0 + at b (3) Exponential law:  = 0 + a[1-exp(-bt)] (4) Logarithmic law:  = 0 + a ln(1+bt) (5) Blackburn’s law:  = 0 + ac[1 - exp(-bt)]+c[1 - exp(-dt)] (6) where  is the strain, 0 is the instantaneous strain on dead weight, t is the elapsed time and a, b, c and d are the parameters characterizing the primary creep region. The a, b, c and d values were called the "scaling fac- tors".21 Figure 5 presents representative results of a re- gression analysis, for the creep at 923 K and 27.75 MPa. The exponential-law and power-law equations did not reproduce the experimental data. Compared to the loga- rithmic-law equation, the Blackburn equation provided a better representation of the experimental creep curve. Therefore, the short-term creep for the P91 heat-resistant steels at low stresses could be described with the Blackburn equation. In order for the creep mechanism of the P91 steels at low stresses to be studied, the instantaneous creep behavior was investigated. The specimens were loaded for 4.3 × 105 s until the strain reached 6 × 10–3. In this case, the dislocations could be expected to move. The stress increased or decreased at various levels that were consequently applied and the instantaneous strain was measured. J. ZHE et al.: SHORT-TERM CREEP OF P91 HEAT-RESISTANT STEELS AT LOW STRESSES ... Materiali in tehnologije / Materials and technology 51 (2017) 5, 843–847 845 MATERIALI IN TEHNOLOGIJE/MATERIALS AND TECHNOLOGY (1967–2017) – 50 LET/50 YEARS Figure 3: Strain/time creep curves for P91 at 923 K and various stresses Figure 4: Strain rate/strain creep curves at 923 K and various stresses Figure 6: Example of instantaneous elongation and contraction upon low stress changes at a high temperature Figure 5: Comparison of experimental data and predicted curves of strain versus time at 923 K and 27.75 MPa Figure 7 presents instantaneous-elongation and con- traction examples upon low changes in the stress of the P91 steels. In the figure, the – was the instantaneous strain under a stress decrease and the + was the in- stantaneous strain under a stress increase. The relationship between the stress increment || and the instantaneous strain |E| is presented in Fig- ure 7. The creep demonstrates a viscous behavior be- cause the absolute values of the instantaneous strain for the load increase were equal to the values for the load decrease. Two types of creep at low stress exist. One is creep controlled by the diffusion including the lattice diffusion creep (Nabarro-Herring type)22 at a high-T and grain boundary diffusion creep (Coble type)22 at an inter- mediate-T. The other is creep associated with dislocation movement including free flight motion (climb con- trolled) and viscous motion (glide controlled)23. When creep is controlled by the diffusion, the creep should be a non-viscous behavior. In this case, the absolute values of the instantaneous strain for a small-load increase should be apparently larger than the values for a small-load decrease. If creep is controlled by free flight motion of dislocation, plastic strain can occur instantaneously when the stress is increased by a small amount. There- fore, creep shows non-viscous behavior. When creep is controlled by the viscous glide of dislocations, instant- aneous plastic strain does not occur even if the applied stress is increase suddenly. Thus, creep shows viscous behavior. In this study, the creep demonstrates a viscous behavior, because non instantaneous strain is observed during the stress increase. It means creep may be con- trolled by the viscous glide of dislocations. Figure 8 gives an example of the anelastic backflow, observed for a high reduction in the stress during the transient-creep stage. Specifically, the helicoidal spring specimen was loaded at 27.75 MPa and 923 K for 120 h and consequently unloaded all the stress for 120 h. Two different parts of the creep strain existed: the anelastic strain was reversible, which is presented with solid double arrows, whereas the plastic strain was irreversible and it is presented with dashed double arrows. Therefore, the instantaneous strain that occurred under a sudden stress change included both elastic and anelastic compo- nents. 4 CONCLUSIONS The short-term creep behavior in the P91 heat-resis- tant steels was investigated using instantaneous-stress- change tests. The results were as follows: 1) The creep deformation consisted of the primary creep stages, but no secondary creep stage was observed. 2) The Blackburn equation could be utilized for the creep-curve description because it provided an im- proved representation of the experimental creep curve. 3) The viscous glide of dislocations might have been the dominant creep mechanism because the creep dis- played a viscous behavior. 4) The short-term creep at a low stress displayed an anelastic behavior. Acknowledgment This project was supported by the National Natural Science Foundation of China (Grant No. 51605330). 5 REFERENCES 1 K. Kimura, Y. Takahashi, ASME 2012 Pressure Vessels & Piping Division Conference, American Society of Mechanical Engineers, 18 (2012) 2, 177, doi:10.1016/0308-0161(93)90110-f 2 K. Maruyama, J. S. Lee, Creep & Fracture in High Temperature Components: Design & Life Assessment Issues, DEStech 3 H. G. Armaki, R. Chen, K. Maruyama, M. Igaras, Premature creep failure in strength enhanced high Cr ferritic steels caused by static recovery of tempered martensite lath structures, Materials Science and Engineering A, 527 (2010) 24–25, 6581–6588, doi:10.1016/ j. Msea. 2010. 07. 037 J. ZHE et al.: SHORT-TERM CREEP OF P91 HEAT-RESISTANT STEELS AT LOW STRESSES ... 846 Materiali in tehnologije / Materials and technology 51 (2017) 5, 843–847 MATERIALI IN TEHNOLOGIJE/MATERIALS AND TECHNOLOGY (1967–2017) – 50 LET/50 YEARS Figure 7: Instantaneous strain at a high temperature (T = 923 K) ver- sus the stress change during P91 steady-state creep Figure 8: Elongation versus time during a high stress reduction with- out an elastic strain 4 O. Prat, J. Garcia, D. Rojas, G. Sauthoff, G. Inden, The role of Laves phase on microstructure evolution and creep strength of novel 9%Cr heat resistant steels, Intermetallics, 32 (2013) 32, 362–372, doi:10.1016/j.internet.2012.08.016 5 L. Kyu-Ho, H. Sung-Min, S. Jae-Hyeok, S. Jin-Yoo, H. Joo-Youl, J. Woo-Sang, Effect of Nb addition on Z-phase formation and creep strength in high-Cr martensitic heat-resistant steels, Materials Characterization, 102 (2015) 2, 79–84, doi:10.1016/j.Matchar. 2014. 12. 028 6 X. Dong, Q. Z. Gao, C. Li, 9Cr-1.7W-0.4Mo-Co Ferritic Heat-Resis- tant Steel Isothermal Aging Microstructural Evolution, Publications, Lancaster, 85 (2008) 1–2, 372–379, doi:10.1016/j.ijpvp. 2007. 06. 006 7 Transactions of Materials and Heat Treatment, 36 (2015) 3, 81–86, doi:10. 1016/j.Msea.2013.09.033 8 K. Kimura, H. Kushima, K. Sawada, Long-term creep deformation property of modified 9Cr–1Mo steel, Materials Science and Engi- neering A, 511 (2009) 18, 58–63, doi:10.1016/j.msea.2008.04.095 9 K. Kimura, Y. Toda, H. Kushima, K. Sawada, Creep strength of high chromium steel with ferrite matrix, International Journal of Pressure Vessels and Piping, 87 (2010) 6, 282–288, doi:10.1016/j.ij2010.03. 016 10 E. M. Haney, F. Dalle, M. Sauzay, L. Vincent, I. Tournié, L. Allais, B. Fournier, Macroscopic results of long-term creep on a modified 9Cr–1Mo steel (T91), Materials Science and Engineering A, 510 (2009) 18, 99–103, doi: 10.1016/ j.msea. 2008. 04.099 11 K. Maruyama, S. 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P. Walsh, Creep of copper: 4–300 K, Materials Science and Engineering A, 147 (1991) 1, 23–32, doi:10.1016/0921-5093(91)90801-s 22 W. D. Nix, Effects of Grain Shape on Nabarro-Herring and Coble Creep Processes, Metals Forum, 4 (1981) 1, 38–43 23 H. Hiroyuki, N. Satoshi, K. Junichi, K. Akihiro, Creep deformation characterization of heat resistant steel by stress change test, International Journal of Pressure Vessels and Piping, 24 (2009) 9, 556–562, doi:10.1016/j.ijpvp.2008.06.003 24 K. Maruyama, S. Karashima, Theorethical Consideration of Measurement of Wor-Hardening and Recovery Rates during high temperature Creep, Trans. Japan Inst. Metals, 16 (1975) 11, 671–678, doi:10.2320/matertrans1960.16.671 J. ZHE et al.: SHORT-TERM CREEP OF P91 HEAT-RESISTANT STEELS AT LOW STRESSES ... Materiali in tehnologije / Materials and technology 51 (2017) 5, 843–847 847 MATERIALI IN TEHNOLOGIJE/MATERIALS AND TECHNOLOGY (1967–2017) – 50 LET/50 YEARS Figure 7 presents instantaneous-elongation and con- traction examples upon low changes in the stress of the P91 steels. In the figure, the – was the instantaneous strain under a stress decrease and the + was the in- stantaneous strain under a stress increase. The relationship between the stress increment || and the instantaneous strain |E| is presented in Fig- ure 7. The creep demonstrates a viscous behavior be- cause the absolute values of the instantaneous strain for the load increase were equal to the values for the load decrease. Two types of creep at low stress exist. One is creep controlled by the diffusion including the lattice diffusion creep (Nabarro-Herring type)22 at a high-T and grain boundary diffusion creep (Coble type)22 at an inter- mediate-T. The other is creep associated with dislocation movement including free flight motion (climb con- trolled) and viscous motion (glide controlled)23. When creep is controlled by the diffusion, the creep should be a non-viscous behavior. In this case, the absolute values of the instantaneous strain for a small-load increase should be apparently larger than the values for a small-load decrease. If creep is controlled by free flight motion of dislocation, plastic strain can occur instantaneously when the stress is increased by a small amount. There- fore, creep shows non-viscous behavior. When creep is controlled by the viscous glide of dislocations, instant- aneous plastic strain does not occur even if the applied stress is increase suddenly. Thus, creep shows viscous behavior. In this study, the creep demonstrates a viscous behavior, because non instantaneous strain is observed during the stress increase. It means creep may be con- trolled by the viscous glide of dislocations. Figure 8 gives an example of the anelastic backflow, observed for a high reduction in the stress during the transient-creep stage. Specifically, the helicoidal spring specimen was loaded at 27.75 MPa and 923 K for 120 h and consequently unloaded all the stress for 120 h. Two different parts of the creep strain existed: the anelastic strain was reversible, which is presented with solid double arrows, whereas the plastic strain was irreversible and it is presented with dashed double arrows. Therefore, the instantaneous strain that occurred under a sudden stress change included both elastic and anelastic compo- nents. 4 CONCLUSIONS The short-term creep behavior in the P91 heat-resis- tant steels was investigated using instantaneous-stress- change tests. 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Materiali in tehnologije / Materials and technology 51 (2017) 5, 843–847 847 MATERIALI IN TEHNOLOGIJE/MATERIALS AND TECHNOLOGY (1967–2017) – 50 LET/50 YEARS