UDK 66.017:519.61/.64:620.17 Original scientific article/Izvirni znanstveni članek ISSN 1580-2949 MTAEC9, 46(2)97(2012) LINEAR TWO-SCALE MODEL FOR DETERMINING THE MECHANICAL PROPERTIES OF A TEXTILE COMPOSITE MATERIAL LINEARNI DVOSTOPENJSKI MODEL ZA DOLOČITEV MEHANSKIH LASTNOSTI TEKSTILNEGA KOMPOZITA Tomaš Kroupa1, Petr Janda2, Robert Zemčik3 1University of West Bohemia in Pilsen, Department of Mechanics, Univerzitni 22, 306 14, Plzen, Czech Republic 2University of West Bohemia in Pilsen, Department of Machine design, Univerzitni 22, 306 14 Plzen, Czech Republic 3University of West Bohemia in Pilsen, Department of Mechanics, Univerzitni 22, 306 14, Plzen, Czech Republic kroupa@kme.zcu.cz Prejem rokopisa - received: 2011-02-01; sprejem za objavo - accepted for publication: 2011-10-10 The engineering mechanical constants for a description of mechanical macro-scale models of carbon and aramid textile composite materials are calculated using finite-element analyses. Two sub-scale models of representative volumes are used. The micro-scale model represents a periodically repeated volume consisting of fibers and a matrix within each interweaved yarn. The meso-scale model represents a unit cell of four interweaved yarns, which is repeated within the whole composite with the properties obtained from a micro-scale model and matrix. The finite-element models are built with the commercial packages Siemens NX 7.5 and MSC.Marc 2008r1 using subroutines. Keywords: composite, textile, linear, carbon, aramid, epoxy, tensile, finite-element analysis Z uporabo metode končnih elementov so izračunane inženirske konstante za opis mehanskega makrodimenzionalnega ogljik-aramidnega modela kompozita. Uporabljena sta dva poddimenzionalna modela za manjše ustrezne prostornine. Mikrodimenzionalni model je periodično ponavljanje prostornine, ki se ponavlja za ves kompozit za matico in vpleteno vlakno. Mezodimenzionalni model je spletna celica iz štirih vpletenih vlaken in se ponavlja v vsem kompozitu z lastnostmi mikromodela in matice. Modeli končnih elementov so vgrajeni v paketa Siemens NX 7.5 in MSC.Marc 2008r1 z uporabo podrutin. Ključne besede: kompozit, tekstil, linearen, ogljik, aramid, epoksi, natezne lastnosti, končni elementi 1 INTRODUCTION A knowledge of the precise values of the mechanical properties of materials is crucial for the capability of models to predict the behavior of analyzed structures. This is also the case for the modeling of composite materials. Several material properties of the composites can be calculated directly from experimental results (Young's moduli from tensile tests, etc.). The presented paper is aimed at a determination of the elasticity constants of textile composites using sub-scale models to determine the properties that cannot be measured and calculated directly from the experiment (shear modulus, etc.). The models were used for the prediction of the elasticity constants of two materials with a simple plain weave. This type of material was chosen because of the possibility to measure directly the Young's moduli in the principal material directions using tensile tests. Nevertheless, the shear modulus was fitted on the linear part of the measured curves using a gradient-optimization algorithm and the Poisson's ratios of the whole textile composites were identified using a digital image correlation1. The material data of the constituents were given by the manufacturer and the dimensions of the periodically repeated volume (unit-cell element - UCE) of the textiles were measured using a digital camera. 2 EXPERIMENT The effective material parameters were determined using simple tensile tests performed on a Zwick/ Roell Z050 test machine on thin strips with the dimensions given in Table 1. Table 1: Dimensions of the strips Tabela 1: Dimenzije traka Carbon Aramid Length mm 100.00 100.00 Width mm 10.00 10.00 Thickness mm 0.30 0.35 Three types of specimens were used for each material. One of two principal directions of the textile fabric form the angles 0°, 45° and 90° with the direction of the loading force. Once the force-displacement diagrams (Figures 1 and 2) were measured, the Young's moduli in directions 1 and 2 and the shear modulus were fitted on the linear parts of the curves using a combination of a plane-stress finite-element (FE) model and the gradient-optimization algorithm implemented in OptiSLang software (the methodology is described in2,3). A digital image correlation1 was used for the calculation Carbon/Epoxy Aramid/Epoxy El GPa 31.05 15.85 E2 GPa 29.73 15.66 Gl2 GPa 1.83 1.24 Vl2 - 0.19 0.31 2 J" 1 Figure 3: Material axes: yarn (left), textile (right) Slika 3: Osi materiala: vlakno (levo), tekstil (desno) Figure 1: Force-displacement diagram (gray) for Carbon/Epoxy, with fitted parts (black) Slika 1: Odvisnost sila - premik (sivo) za ogljik/epoksi s približki (črno) Figure 2: Force-displacement diagrams (gray) for Aramid/Epoxy, with fitted parts (black) Slika 2: Odvisnost sila - premik (sivo) za aramid/epoksi s približki (črno) of the Poisson's ratios. The elasticity parameters of the textiles are shown in Table 2. Table 2: Elasticity parameters of textile composites Tabela 2: Parametri elastičnosti za tekstilne kompozite Figure 4: UCE geometry of yarn with Vf = 0.6 (fibers - black, matrix - gray) Slika 4: UCE-geometrija vlakna z Vf = 0.6 (vlakna - črno, matica -sivo) Table 3: Dimensions of the unit cell of the yarn Tabela 3: Dimenzije spletne celice l1 [-1 1 l2 [-1 4 l3 [-1 4 3 UNIT-CELL ELEMENTS Axes orientations in UCE (Figure 4) are shown in Figure 3. Dimensionless geometry of UCE of yarns is shown in Table 3. The ideal distribution of fibers in the yarns, the perfect saturation of the yarns by the matrix and the volume fiber fractions Vf = 0.6 and Vf = 0.7 are considered in the calculations. Figure 5: Photograph of Carbon/Epoxy specimen Slika 5: Posnetek vzorca ogljik/epoksi B [wb .WB ] Figure 6: Photograph of Aramid/Epoxy specimen Slika 6: Posnetek vzorca aramid/epoksi The dimensions of the UCE of both materials, which were measured using detailed photographs provided by a Canon EOS 400D digital camera (Figures 5 and 6) are shown in Table 4. Table 4: Dimensions of textile unit cells Tabela 4: Dimenzije spletne celice tekstila mm mm mm Carbon/Epoxy .5.00 5.00 0.30 Aramid/Epoxy 3.00 3.00 0.3.5 4 BOUNDARY CONDITIONS In the FE model of the UCE (Figure 7) it is necessary to invoke pure tensile conditions or pure shear conditions to determine the elasticity parameters. Furthermore, the UCE has to be fixed in space to eliminate rigid body modes. Finally, the periodic boundary conditions have to be satisfied. The effect of the periodic boundary condition on the UCE with two periodically tied faces is sketched in Figure 8. Figure 8: Scheme of the effect of the periodic boundary conditions Slika 8: Shema učinka periodičnosti mejnih pogojev Each corresponding pair of nodes on opposite faces of the FE model must fulfill the conditions 4-6 -u A = du, V B - V A = dv = di for i=\...N Ub-UA wl -w (P) where i is the index of the corresponding constrained faces; N is the total number of the periodically constrained faces; u, v and w are the displacements in the 1, 2 and 3 direction; and d'u, dV, dWw are displacements of the appropriate retained nodes in which the loading is applied (Figure 9). The UCE of the yarns is periodically tied in all three directions and the UCE of the textiles is tied in direction 1 and 2 (Figure 9). For the determination of the Young's modulus E1 and the Poisson's ratio Vi2 of the textile composite the model is loaded with Oi ^ 0 and the other loadings are equal to zero. Normal strains in direction 1 and 2 are calculated as d; d22 = , £2 = (e12) h '2 and the Young's modulus and Poisson's ratio are E„ E, = (E1v12) Figure 7: UCE geometry of Carbon/Epoxy textile composite (yarns -black, matrix - gray) Slika 7: UCE-geometrija kompozita ogljik/epoksi (trakovi - črno, matica - sivo) Figure 9: Boundary conditions and links used for periodic boundary conditions for UCE of Aramid/Epoxy textile Slika 9: Mejni pogoji in povezave, uporabljene za periodične mejne pogoje za UCE aramid/epoksi tekstil 1 For the determination of the shear modulus G12 the model is loaded by 712 ^ 0. The other loadings are equal to zero. The shear strain in plane 12 is calculated as y 12 = and the shear modulus is d 2 I1 I2 G12 = y 1 (g12) (G12) The same scheme is used for the determination of the elasticity constants in the other directions or planes. 5 INPUT PARAMETERS Carbon (Toray T600) and Aramid (Twaron K1055) fibers are transversely isotropic materials. Their elasticity parameters are given in Table 5. Table 5: Elasticity parameters for fibers Tabela 5: Parametri elasti~nosti za vlakna Carbon Aramid E1 GPa 230.00 104.00 E2 GPa 7.05 5.40 E3 GPa 7.05 5.40 V12 - 0.30 0.40 V23 - 0.30 0.40 V31 - 0.02 0.02 G12 GPa 50.00 12.00 G23 GPa 50.00 12.00 G31 GPa 50.00 12.00 Figure 11: Deformed FE model of the UCE of the textile under shear loading in plane 12 (shown values of shear stress r12) Slika 11: Deformiran FE-model UCE za tekstil pri strižni obremenitvi v ravnini 12 (prikazane vrednosti strižne napetosti r12) Table 6: Elasticity parameters for the matrix Tabela 6: Parametri elasti~nosti za matico Epoxy E GPa 3.00 v - 0.30 The matrix is manufactured from epoxy resin (MGS® L 285) and hardener (MGS® 285). It is considered to be a linear isotropic material (Table 6). 6 RESULTS The effect of the periodic boundary conditions is shown in Figures 10 and 11. Opposite faces of the UCE are deformed in the same shape. The elastic properties of the yarns are shown in Table 7. The results are shown for both fiber volume fractions (Vf). Similarly, the results for the textiles are shown for both Vf (Table 8). Table 7: Calculated elasticity parameters of the yarns Tabela 7: Izra~unani parametri elasti~nosti za spleta Figure 10: Deformed FE model of the UCE of yarn under shear loading in plane 23 (shown values of shear stress r23) Slika 10: Deformiran FE-model za UCE-spleta pri strižni obremenitvi v ravnini 23 (prikazane vrednosti strižne napetosti r23) Carbon/Epoxy Aramid/Epoxy Vf - 0.60 0.70 0.60 0.70 E1 GPa 138.87 161.54 63.46 73.55 E2 GPa 7.05 8.33 4.36 4.60 E3 GPa 7.05 8.33 4.36 4.60 v12 - 0.30 0.30 0.36 0.37 v23 - 0.36 0.34 0.40 0.40 v31 - 0.02 0.02 0.02 0.02 G12 GPa 4.26 5.90 3.42 4.34 G23 GPa 3.88 5.45 3.15 4.01 G31 GPa 4.26 5.90 3.42 4.34 Table 8: Calculated elasticity parameters for textiles Tabela 8: Izra~unani parametri elasti~nosti za tekstil Carbon/Epoxy Aramid/Epoxy Vf - 0.60 0.70 0.60 0.70 E1 GPa 27.75 31.89 14.08 15.72 E2 GPa 27.75 31.89 14.08 15.72 G12 GPa 2.60 3.30 2.21 2.60 v12 - 0.33 0.33 0.28 0.29 2 12 7 CONCLUSION Multi-scale models for the prediction of the elasticity constants of textile composites with a simple plain weave were developed and presented. Good agreement of the Young's moduli was achieved between the calculated and experimental values. However, the shear moduli are slightly over-predicted. The calculated Poisson's ratios were calculated with acceptable accuracy only for the Aramid/Epoxy textile. Future research will be aimed at the non-linear, plastic and damage behavior of the matrix, the damage behavior of the fibers and an investigation of the imperfections and the unit-cell element dimensions of the textiles. Acknowledgement The work has been supported by the projects GA P101/11/0288 and European project NTIS - New Technologies for Information Society No. CZ.1.05/ 1.1.00/02.0090. 8 REFERENCES 1 R. Kottner, R. Zemcik, V. Las, Mechanical characteristics of rubber segment - shear test. In: Experimental Stress Analysis 2007 2T. Kroupa, R. Zemcik, J. Klepacek, Temperature dependence of parameters of non-linear stress-strain relations for carbon epoxy composites, Mater. Tehnol., 43 (2009) 2, 69-72 3T. Kroupa, R. 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